Shear Bond Strength of Composite Resin Attachments in Clear Aligner Orthodontic Appliances with Different Adhesive Systems

Objectives: Orthodontic treatments with clear aligners are popular. Loss of composite resin attachments during treatment remains a concern. Self-adhesive composite resins were introduced to simplify bonding. This study compared the shear bond strength (SBS) and evaluated the failure modes of self-adhesive and conventional composite resin.

Methods: Eighty-four intact upper first premolars were used, 80 were randomly allocated into five groups with different bonding protocols: Group 1 (etch and rinse + conventional flowable composite resin), Group 2 (self-etching + conventional flowable composite resin), Group 3 (self-adhesive composite resin), Group 4 (etching + self-adhesive composite resin), and Group 5 (self-etching + self-adhesive composite resin). After thermocycling, the SBS was tested using a universal testing machine and analyzed with one-way ANOVA (p<0.05). Failure modes were determined under a stereomicroscope. The enamel surface of four unallocated teeth with different preparations were assessed by a scanning electron microscope.

Results: 62.5% of attachments in Group 3 dislodged after thermocycling. The mean SBS (MPa) was significantly higher in Group 1 (17.72±5.37), Group 2 (19.13±5.37), Group 4 (19.03±6.91), and Group 5 (13.21±4.87) than in Group 3 (3.69±1.30); (p<0.05). Most failures in Groups 1, 2, 4, and 5 were mixed, while Group 3 exhibited only adhesive failure.

Conclusions: Self-adhesive composite resin alone had the lowest SBS. Pretreatment with 37% phosphoric acid or a self-etching primer significantly improved the SBS.

References

1. Weir T. Clear aligners in orthodontic treatment. Aust Dent J. 2017;62:58-62.

2. Jedliński M, Mazur M, Greco M, Belfus J, Grocholewicz K, Janiszewska-Olszowska J. Attachments for the orthodontic aligner treatment-state of the art-a comprehensive systematic review. Int J Environ Res Public Health. 2023;20(5):4481.

3. Yaosen C, Mohamed AM, Jinbo W, Ziwei Z, Al-Balaa M, Yan Y. Risk factors of composite attachment loss in orthodontic patients during orthodontic clear aligner therapy: a prospective study. Biomed Res Int. 2021. 2021:6620377.

4. Alshammari RR, Alshihah N, Aldweesh A. Mechanical properties of different types of composite resin used as clear aligner attachments: an in vitro study. Saudi Dent J. 2025;37(4-6):12.

5. Ocak I, Gorucu-Coskuner H, Aksu M. Wear resistance of orthodontic attachments: a comparative analysis of different composite resins in clear aligner therapy. Clin Oral Investig. 2025;29(5):242.

6. Dasy H, Dasy A, Asatrian G, Rózsa N, Lee HF, Kwak JH. Effects of variable attachment shapes and aligner material on aligner retention. Angle Orthod. 2015;85(6):934-40.

7. Nucera R, Dolci C, Bellocchio AM, Costa S, Barbera S, Rustico L, et al. Effects of composite attachments on orthodontic clear aligners therapy: a systematic review. Materials (Basel). 2022;15(2):533.

8. Bayram M, Yeşilyurt C, Kuşgöz A, Ülker M, Nur M. Shear bond strength of orthodontic brackets to aged resin composite surfaces: effect of surface conditioning. Eur J Orthod. 2010;33(2):174-9.

9. Al Noor HSS, Al-Joubori SK. Retention of different orthodontic aligners according to their thickness and the presence of attachments. Int J Med Res Health Sci. 2018;7(11):115-21.

10. Reynolds IR. A Review of direct orthodontic bonding. Br J Orthod. 1975;2(3):171-8.

11. Ozer F, Blatz MB. Self-etch and etch-and-rinse adhesive systems in clinical dentistry. Compend Contin Educ Dent. 2013;34(1):12-4, 16, 18; quiz 20, 30.

12. Valizadeh S, Alimohammadi G, Nik TH, Etemadi A, Tanbakuchi B. In vitro evaluation of shear bond strength of orthodontic metal brackets to aged composite using a self-adhesive composite: effect of surface conditioning and different bonding agents. Int Orthod. 2020;18(3):528-37.

13. Tosun G, Sener Y, Sengun A. Effect of storage duration/ solution on microshear bond strength of composite to enamel. Dent Mater J. 2007;26(1):116-21.

14. Lee JJ, Nettey-Marbell A, Cook A, Jr., Pimenta LA, Leonard R, Ritter AV. Using extracted teeth for research: the effect of storage medium and sterilization on dentin bond strengths. J Am Dent Assoc. 2007;138(12):1599-603.

15. Goracci C, Margvelashvili M, Giovannetti A, Vichi A, Ferrari M. Shear bond strength of orthodontic brackets bonded with a new self-adhering flowable resin composite. Clin Oral Investig. 2013;17(2):609-17.

16. Årtun J, Bergland S. Clinical trials with crystal growth conditioning as an alternative to acid-etch enamel pretreatment. Am J Orthod. 1984;85(4):333-40.

17. Chen W, Qian L, Qian Y, Zhang Z, Wen X. Comparative study of three composite materials in bonding attachments for clear aligners. Orthod Craniofac Res. 2021;24(4):520-7.

18. Sabbagh J, Dagher S, El Osta N, Souhaid P. Randomized clinical trial of a self-adhering flowable composite for Class I restorations: 2-year results. Int J Dent. 2017;2017:5041529.

19. Elraggal A, Raheem IA, Holiel A, Alhotan A, Alshabib A, Silikas N, et al. Bond strength, microleakage, microgaps, and marginal adaptation of self-adhesive resin composites to tooth substrates with and without preconditioning with universal adhesives. J Adhes Dent. 2024;26:53-64.

20. Veli I, Akin M, Kucukyilmaz E, Uysal T. Shear bond strength of a self-adhering flowable composite when used for lingual retainer bonding. J Orofac Orthop. 2014;75(5):374-83.

21. Talan J, Gupta S, Nikhil V, Jaiswal S. Effect of mechanical alteration of enamel surface on shear bond strength of different bonding techniques. J Conserv Dent. 2020;23(2):141-4.

22. Dunnett CW. Pairwise multiple comparisons in the unequal variance case. J Am Stat Assoc. 1980;75(372):796-800.

23. Lamper T, Ilie N, Huth KC, Rudzki I, Wichelhaus A, Paschos E. Self-etch adhesives for the bonding of orthodontic brackets: faster, stronger, safer?. Clin Oral Investig. 2014;18(1):313-9.

24. Sandhu SV, Tiwari R, Bhullar RK, Bansal H, Bhandari R, Kakkar T, et al. Sterilization of extracted human teeth: a comparative analysis. J Oral Biol Craniofac Res. 2012;2(3):170-5.

25. Kohn WG, Collins AS, Cleveland JL, Harte JA, Eklund KJ, Malvitz DM. Guidelines for infection control in dental health-care settings-2003. MMWR Recomm Rep. 2003;52(RR-17):1-61.

26. Sibai N, El Mourad A, Al Suhaibani N, Al Ahmadi R, Al Dosary S. Shear bond strength of self-adhesive flowable resin composite. Int J Dent. 2022;2022:1-8.

27. Meharry MR, Moazzami SM, Li Y. Comparison of enamel and dentin shear bond strengths of current dental bonding adhesives from three bond generations. Oper Dent. 2013;38(6):E237-45.

Thongkom S, Khemaleelakun W, Sirabanchongkran S. Shear Bond Strength of Composite Resin Attachments in Clear Aligner Orthodontic Appliances with Different Adhesive Systems: Original articles. Oral Sci Rep [Internet]. 2025 Dec 17 [cited 2025 Dec 17];47(1):95-102. Available from: https://www.dent.cmu.ac.th/cmdj/frontend/web/?r=site/viewarticle&id=534

Thongkom, S., Khemaleelakun, W. & Sirabanchongkran, S. (2025). Shear Bond Strength of Composite Resin Attachments in Clear Aligner Orthodontic Appliances with Different Adhesive Systems. Oral Sci Rep, 47(1), 95-102. Retrieved from: https://www.dent.cmu.ac.th/cmdj/frontend/web/?r=site/viewarticle&id=534

Thongkom, S., Wikanda Khemaleelakun and Supassara Sirabanchongkran. 2025. "Shear Bond Strength of Composite Resin Attachments in Clear Aligner Orthodontic Appliances with Different Adhesive Systems." Oral Sci Rep, 47(1), 95-102. https://www.dent.cmu.ac.th/cmdj/frontend/web/?r=site/viewarticle&id=534

Thongkom, S. et al. 2025. 'Shear Bond Strength of Composite Resin Attachments in Clear Aligner Orthodontic Appliances with Different Adhesive Systems', Oral Sci Rep, 47(1), 95-102. Retrieved from https://www.dent.cmu.ac.th/cmdj/frontend/web/?r=site/viewarticle&id=534

Thongkom, S., Khemaleelakun, W. and Sirabanchongkran, S. "Shear Bond Strength of Composite Resin Attachments in Clear Aligner Orthodontic Appliances with Different Adhesive Systems", Oral Sci Rep, vol.47, no. 1, pp. 95-102, Dec. 2025.

Siriwan Thongkom, Wikanda Khemaleelakun, Supassara Sirabanchongkran "Shear Bond Strength of Composite Resin Attachments in Clear Aligner Orthodontic Appliances with Different Adhesive Systems." Oral Sci Rep, vol.47, no. 1, Dec. 2025, pp. 95-102, https://www.dent.cmu.ac.th/cmdj/frontend/web/?r=site/viewarticle&id=534