Comparison of Bonding Efficiency Between Flowable Composite Core and Fiber-reinforced Composite Post Which Surface Treatment with Silane Coupling Agent and Plasma Jet

The purpose of this study was to investigate the bond strength of fiber-reinforced composite post to flowable composite core build-up material after air plasma jet surface treatment. Fifty six DT Light-Post® were divided into 4 groups according to surface treatment: i. untreated surface group (control), ii. silane coupling agent treated surface group, iii. air mixed with helium plasma jet treated surface group, and iv. air mixed with argon plasma jet treated surface group. The coronal parts of the fiber posts were encapsulated with flowable composite core build-up material. The specimens were immersed in distilled water at 37°C for 24 hours. All specimens were pull-out tests by using a universal testing machine to evaluate the tensile-shear bond strength of the specimens in each group (n = 8). Profilometer and scanning electron microscope were used to examine the surface roughness and surface morphology in the non-encapsulated flowable composite posts (n= 2). Fourier transform infrared spectroscopy was used to measure the functional group in the posts after surface treatments (n=2). One-way ANOVA and Tamhane’s multiple comparisons test revealed that there were no significant differences in tensile-shear bond strengths among each group (p=0.05). No significant differences were found in the surface roughness of all post specimens with Tukeyís test (p = 0.05).

1. Duret B, Duret F, Reynaud M. Long-life physical property preservation and postendodontic rehabilitation with the composipost. Compend Contin Educ Dent Compend Contin Educ Dent 1996; suppl. No 1996; suppl. No 20: s50-56.

2. Monticelli F, Grandini S, Goracci C, Ferrari M. Clinical behavior of translucent-fiber posts: a 2-years prospective study. Int J Prosthodont 2003; 16: 593-596.

3. Baldissara P, Zicari F, Valandro LF, Scotti R. Effect of root canal treatments on quartz fiber posts bonding to root posts bonding to root dentin. dentin. J Endod J Endod 2006; 32: 985-988.

4. Perdigao J, Gomes G, Lee IK. The effect of silane on the bond strengths of fiber posts. Dent Mater 2006; 22: 752-758.

5. Aksornmuang J, Foxton RM, Nakajima M, Tagami J. Microtensile bond strength of a dual-cure resin core material to glass and quartz fiber posts. J Dent 2004; 32: 433-450.

6. Ozcan M, Vallittu PK. Effect of surface conditioning methods on the bond strength of luting cements to ceramics. Dent Mater 2003; 19: 725-731.

7. Sahafi A, Peutzfeldt A, Asmussen E, Gotfredsen K. Effect of surface treatment of prefabricated posts on bonding of resin cement. Oper Dent 2004; 29: 60-68.

8. Goracci C, Raffaelli O, Monticelli F, Balleri B, Bertelli E, Ferrari M. The adhesion between prefabricated FRC posts and composite resin cores: microtensile bond strength with and without post-silanization. Dent Mater Dent Mater 2005; 21: 437-444.

9. Vano M, Goracci C, Monticelli F, Tognini F, Tay FR, Ferrari M. The adhesion between fiber posts and composite resin cores: the evaluation of microtensile bond strength following various surface chemical treatments to posts. Int Endod J 2006; 39: 31-39.

10. Sahifi A, Peutzfeldt A, Asmussen E, Gotfredsen K. Bond strength of sen K. Bond strength of resin cement to resin cement to surface-treated posts of titanium alloy, glass fiber, and zirconia, and to dentin. J Adhes Dent 2003; 5: 153-162.

11. Yavirach P, Chaijareenont P, Boonyawan D, et al. Effects of plasma treatment on the shear bond strength between fiber-reinforced composite posts and resin composite for core buildup. Dent Mater 2009; 28: 686-692.

12. Goracci C, Tavares AU, Fabianelli A, et al. The adhesion between fiber posts and root canal walls: comparison between microtensile and push-out bond strength measurements. Eur J Oral Sci 2004; 112: 353-361.

13. Matinlinna JP, Lassila LV, Vallittu PK. Evaluation of five silanes on bonding a luting cement onto silica-coated titanium. J Dent 2006; 34: 721-726.

14. Matinlinna JP, Lassila LVJ, Ozcan M, YliUrpo A, Vallittu PK. An introduction to silanes and their clinical applications in Dentistry. Int J Prosthodont 2004; 17: 155-164.

15. Cvelbar U, Pejovnik S, Mozetie M, Zalar A. Increased surface roughness by oxygen plasma treatment of graphite/polymer composite. Appl Surf Sci 2003; 210: 255-261.

16. ศรีเพ็ญ ท้าวตก กระบวนการผลิตพลาสมาเพื่อปรับเปลี่ยนสมบัติของสิ่งทอ วิทยาศาสตร์มหาบัณฑิต มหาวิทยาลัยเชียงใหม่ มหาวิทยาลัยเชียงใหม่, 2547.

17. Derand T, Molin M, Kvam K. Bond strength of composite luting cement to zirconia ceramic surfaces. Dent Mater 2005; 21: 1158-1162.

18. Liston EM, Martinu L, Wertheimer MR. Plasma surface modification of polymers for improved adhesion: a critical review. J Adhesion Sci Technol 1993; 7: 1091-1127.

19. Lai J, Sunderland B, Xue J, et al. Study on hydrophilicity of polymer surfaces improved by plasma treatment. Appl Surf Sci 2006; 252: 3375-3379.

20. Grace JM, Gerenser LJ. Plasma treatment of polymers. J dispersion Sci Technol J dispersion Sci Technol 2003; 24: 2003; 24: 305-341.

21. Inagaki N. Plasma surface modification and polymer chain ends. J Vac Soc Jpn 2007; 50: 625-628.

22. Yavirach P, Duangsuriya S,Sermchaiwong U. Shear-Bond Strength Between Heat-Polymerized Acrylic Resin Within Different Surface Treatments and Autopolymerized Acrylic Resin. CM Dent J 2011; 32(2): 93-101.

23. Kanazawa S, Kogoma M, Moriwaki T, Okazaki S. Stable glow plasma at atmospheric pressure. J Phys Appl Phys 1988; 21: 838-840.

24. Noeske M, Degenhardt J, Struthoff S, Lommatzsch U. Plasma jet treatment of five polymers at atmospheric pressure: surface modifications and the relevance for adhesion. Int J Adhes Adhes 2004; 24: 171-177.

25. Hicks RF. Atmospheric-pressure plasma cleaning of contaminated surfaces. University of California, Los Angeles; 1999: 1-131.

26. Nishigawa G, Maruo Y, Oka M, Oki K, Minagi S, Okamoto M. Plasma treatment increased shear bond strength between heat-cured acrylic resin and self-curing acrylic resin. J Oral Rehabil 2003; 30: 1081-1084.

27. Walsh JL, Shi JJ, Kong MG. Contrasting characteristics of pulsed characteristics of pulsed and sinusoidal cold and sinusoidal cold atmospheric plasma jets. Appl Phys Lett Appl Phys Lett 2006; 88: 171501-171503.

28. Debnath S, Wunder SL, McCool JL, Baran GR. Silane treatment effects on glass resin interfacial shear strength. Dent Mater Dent Mater 2003; 19: 441-448.

29. Lommatzsch U, Pasedag D, Baalmann A, Ellinghorst G, Wagner H-E. Atmospheric pressure plasma jet treatment of polyethylene surfaces for adhesion improvement. Plasma Process and Polymer 2007; 4: s1041-s1045.

30. Hong YC, Uhm HS. Air plasma jet with hallow electrodes at atmospheric pressure. Phys Plasma 2007; 14: 053503-053505.

31. Riccardi C, Barni R, Selli E, et al. Surface modification of poly (ethylene terepthalate) fibers induced by radio frequency air plasma treatment. Appl Surf Sci 2003; 211: 386-397.

32. Boenig HV. Plasma Science and Technology. New York: Cornell Press: Ithanica; 1982.

33. Wei QF, Gao WD, Hou DY, Wang XQ. Surface modification of polymer nanofibers by plasma treatment. Appl Surf Sci 2005; 245: 16-20.

34. Castro Vidaurre EF, Achete CA, Gallo F, Garcia D, Simao R, Habert AC. Surface modification of polymeric materials by plasma treatment. Materials Research 2001; 5: 37-41.

35. Rusu IA, Borcia G, Sayed SO, Sullivan JL. Arf plasma effect on polymer surface. Paper read at 28th ICPIG. 15-20 July2007, at Prague, Czech Republic.

36. Arefi-Khonsari F, Tatoulian M. Plasma processing of polymers by a low-frequency discharge with asymmetrical configuration of electrodes. In: Advanced plasma technology, Willey-VCH Verlag GmbH & Co. KGaA, Germany; 2008: 137-174.

37. Cheng C, Liye Z, Zhan RJ. Surface modification of polymer fiber by the new atmospheric pressure cold plasma jet. Surf Coat Technol 2006; 200: 6659-6665.

38. Loyaga-Rendon PG, Takahashi H, Iwasaki N, Reza F. Effect of ultraviolet light irradiation on bonding of experimental composite resin artificial teeth. Dent Mater 2007; 26: 805-813.

39. Ye H, Zhang Q, Sun K, Zhang J, Jiao Y, Zhou Y. Aging effect of fiber post surface treatment with nonthermal plasma. Int J Prosthodont 2012; 25: 509-511.


Yavirach P, Chaijareenont P, Chinsawananon S, Rungsiyakull P, Silthampitag P, Boonyawan D. Comparison of Bonding Efficiency Between Flowable Composite Core and Fiber-reinforced Composite Post Which Surface Treatment with Silane Coupling Agent and Plasma Jet: Original articles. CM Dent J [Internet]. 2024 Dec 04 [cited 2025 May 03];34(1):91-106. Available from: https://www.dent.cmu.ac.th/cmdj/frontend/web/?r=site/viewarticle&id=323

Yavirach, P., Chaijareenont, P., Chinsawananon, S., Rungsiyakull, P., Silthampitag, P. & Boonyawan, D. (2024). Comparison of Bonding Efficiency Between Flowable Composite Core and Fiber-reinforced Composite Post Which Surface Treatment with Silane Coupling Agent and Plasma Jet. CM Dent J, 34(1), 91-106. Retrieved from: https://www.dent.cmu.ac.th/cmdj/frontend/web/?r=site/viewarticle&id=323

Yavirach, P., Pisaisit Chaijareenont,Sonchanin Chinsawananon,Pimduen Rungsiyakull,Patcharawan Silthampitag and Dheerawan Boonyawan. 2024. "Comparison of Bonding Efficiency Between Flowable Composite Core and Fiber-reinforced Composite Post Which Surface Treatment with Silane Coupling Agent and Plasma Jet." CM Dent J, 34(1), 91-106. https://www.dent.cmu.ac.th/cmdj/frontend/web/?r=site/viewarticle&id=323

Yavirach, P. et al. 2024. 'Comparison of Bonding Efficiency Between Flowable Composite Core and Fiber-reinforced Composite Post Which Surface Treatment with Silane Coupling Agent and Plasma Jet', CM Dent J, 34(1), 91-106. Retrieved from https://www.dent.cmu.ac.th/cmdj/frontend/web/?r=site/viewarticle&id=323

Yavirach, P., Chaijareenont, P., Chinsawananon, S., Rungsiyakull, P., Silthampitag, P. and Boonyawan, D. "Comparison of Bonding Efficiency Between Flowable Composite Core and Fiber-reinforced Composite Post Which Surface Treatment with Silane Coupling Agent and Plasma Jet", CM Dent J, vol.34, no. 1, pp. 91-106, Dec. 2024.

Yavirach, P., Chaijareenont, P., Chinsawananon, S., et al. "Comparison of Bonding Efficiency Between Flowable Composite Core and Fiber-reinforced Composite Post Which Surface Treatment with Silane Coupling Agent and Plasma Jet." CM Dent J, vol.34, no. 1, Dec. 2024, pp. 91-106, https://www.dent.cmu.ac.th/cmdj/frontend/web/?r=site/viewarticle&id=323